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All data were lock mass corrected on the pentapeptide leucine enkephaline (Tyr-Gly-Gly-Phe-Leu, m/z 556.2771, [M+H] + and m/z 554.2615, [M-H] ) in a solution (2 ng/L) of MeCN/0.1% HCO 2 H (1/1, v/v)